/ Home
/ SUBMISSION

/ The BJOC
/ Diamond Open Access
/ Journal Statistics
/ Editorial Board
/ Community
/ Call for papers

/ Latest Articles
/ Most accessed
/ Thematic issues
/ Volumes
/ Authors

/ Alerts

/ TWITTER
/ LINKEDIN
/ Mastodon
/ RSS FEED

Empty search

Article Type

Publication Date Range

Search Tips

This search combines search strings from the content search (i.e. "Full Text", "Author", "Title", "Abstract", or "Keywords") with "Article Type" and "Publication Date Range" using the AND operator.

Search Examples

aromatic	the word “aromatic”
aromatic aldehyde	the word “aromatic” OR “aldehyde”
+aromatic +aldehyde	both words “aromatic” AND “aldehyde”
+aromatic -aldehyde	the word “aromatic” but NOT “aldehyde”
“aromatic aldehyde”	the exact phrase “aromatic aldehyde”
benz*	words which begin with “benz”, such as “benzene” or “benzyl”
benz*yl	words that begin with “benz” and end with “yl”, such as “benzyl” or “benzoyl”
benzyl~	words that are close to the word “benzyl”, such as “benzoyl” (i.e., fuzzy search)

BROWSE
Latest Articles
Most accessed
thematic issues
volumes
authors

BROWSE

Latest Articles Most Accessed Thematic Issues Volumes Authors

Author

1 article(s) from Sunil Kumar, I V

Identification and synthesis of impurities formed during sertindole preparation

I. V. Sunil Kumar,
G. S. R. Anjaneyulu and
V. Hima Bindu

Beilstein J. Org. Chem. 2011, 7, 29–33, doi:10.3762/bjoc.7.5

PDF

Graphical Abstract

Figure 1: Sertindole (1), process related impurities and metabolites.

Jump to Figure 1

Scheme 1: Reagents and conditions: i) K₂CO₃, CuBr, ethylenediamine, DMF 130–135 °C; ii) CH₃COOH, CF₃COOH, 100...

Jump to Scheme 1

Scheme 2: Reagents, conditions (and yields): i) (a) pH adjusted to 6; (b) Pd/C, HCOONH₄, AcOH, MeOH, reflux (...

Jump to Scheme 2

Scheme 3: Reagents, conditions (and yields): i) 16, K₂CO₃, KI, MIBK, reflux (73.9%).

Jump to Scheme 3

Scheme 4: Reagents, conditions (and yields): i) Cs₂CO₃, DMF, 130–135 °C; ii) 14, CH₃COOH, CF₃COOH, 100–105 °C...

Jump to Scheme 4

Scheme 5: Reagents, conditions (and yields): i) (a) pH adjusted to 6–7; (b) H₂, PtO₂, MeOH, AcOH, 30–35 °C (7...

Jump to Scheme 5

Scheme 6: Reagents, conditions (and yields): i) 12, K₂CO₃, Cu(II)Br, ethylenediamine, DMF, 130–135 °C, (51%);...

Jump to Scheme 6

Scheme 7: Reagents, conditions (and yield): i) (a) 16, Et₃N, NaI, CH₃CN, reflux; (b) column chromatography (1...

Jump to Scheme 7

Scheme 8: Reagents, conditions (and yield): i) (a) mCPBA, MeOH, 40–45 °C; (b) column chromatography (52.2%).

Jump to Scheme 8

Album

Supp Info

Full Research Paper

Published 07 Jan 2011

Full text

Other Beilstein-Institut Open Science Activities

/ Help / Support & Contact / Alerts / Privacy Policy / Terms & Conditions / Impressum